Subject · Mining engineering
Dağ-mədən işlərində analitik nəzarətTopics
Topic plan
The subject's topics and the learning outcomes attached to each one.
1. Introduction. qualified, quantitative, technical, urgent, etc. analyses. standards, technical conditions.
LectureThe object and tasks of analytical chemistry. differences in types of analysis (qualitative, quantitative, technical, etc.). the regulatory role of state standards and technical conditions in the analysis of substances.
2. Antenanın əsas paramertlərinin təcrübi təyini metodları
LectureAntenanın istiqamətlənmə diaqramı, güclənmə əmsalı, faydalı iş əmsalı və digər əsas parametrlərin eksperimental ölçülmə üsulları araşdırılır.
3. Titrimetric analysis: neutralization, oxidation-reduction and complexation.
LectureNeutralization, oxidation-reduction, complexation, etc. methods of analysis. conducting the titration process, finding the equivalence point and calculating the results of the analysis
4. Analytical calculations: determination of concentration and solutions.
LectureMethod without standard, method of comparison with standard, graphical method, etc. determination of concentration with calculating the results of weight analysis using the standard-free method. preparation of solutions with normal, percentage, molar, and titrated concentrations.
5. Electrochemical and radiometric analysis methods.
LectureClassification of electrochemical, optical and radiometric analysis methods. potentiometric, polarographic, electrogravimetric, conductometric, etc. working principles of analytical methods and application in industry.
6. Optical analyzes and spectral properties of the atom.
LectureRefractometric, atomic absorption, nephelometric analysis methods. the essence of characteristic, polychromatic, monochromatic and resonant rays. the structure of the atom, energy levels, energy of the beam, etc.
7. Sample management: preparation of primary and secondary samples.
LectureRules for taking an initial sample, preparation of an average sample. the process of selecting a suitable solvent for the initial sample and dissolving the sample in that selected solvent.
8. Analysis of production materials.
LectureCharacteristics of raw materials, auxiliary materials, waste and finished products and their analysis in industrial conditions.
9. Separation of elements and complex compounds.
LecturePrecipitation in the form of fractions, selective precipitation, chromatography, extraction, etc. separation of elements by methods. conversion of the ion to be determined into a complex compound form and dissociation of the complex ion.
10. An introduction to the science of metrology.
LectureThe basics of metrology science. measurement, measurement tools, determination of standards and a unified system of measurement units.
11. Metrological basis of analysis.
LectureMetrological basis of analysis. measurement differences of absolute and relative methods of analysis. distributed graph. application of external standards method in the calibration process.
12. Measurement errors and measurement accuracy.
LectureRandom, gross and systematic errors and their variance. uncertainties in measurements, measurement accuracy. choosing a confidence interval. analysis of the probability that the results of the analysis are correct.
13. Investigation of systematic errors.
LectureSystematic error distribution mechanisms. detection and investigation of errors occurring at separate stages of analysis (sampling, preparation, hardware error).
14. True and average value of measurement, dispersion of results.
LectureRules for calculating the true or average value of the measurement. the tendency of individual measurement results to deviate from the true value. extraction of the absolute variance of measurement results.
15. Mathematical-statistical processing of the results of the analysis.
LectureProbability in examining the results of the analysis by mathematical and statistical methods. examination of the results on the gaussian function (normal distribution) and graphical representation of error patterns.