Analytical chemistry and instrumental analysisSyllabus

Subject code

İF-3039

Credits

4

Student workload

120

Semester

Autumn semester

Academic year

—

Subject type

Elective

Form of education

Full-time

Language of instruction

Azerbaijani

The subject of analytical chemistry and instrumental analysis in the specialty of ecological engineering teaches qualitative and quantitative analysis of the chemical composition of environmental samples. the subject provides students with theoretical knowledge and practical skills in the application of classical and instrumental analysis methods, use of laboratory equipment and evaluation of analysis results.

• lecture
• laboratory work

1. 1

   CLO 1: Explains the basic concepts, methods and theoretical principles of analytical chemistry.

2. 2

   CLO 2: Evaluating the efficiency of mass and heat transfer processes in the chemical industry from a technical, economic and energy point of view, prepares justified proposals for process optimization.

3. 3

   CLO 3: • ftn2: azərbaycan tarixi üzrə bəzi mübahisəli məsələlərə aydınlıq gətirilir.

4. 4

   CLO 4: Performs sampling, preparation and measurement processes correctly for analysis.

5. 5

   CLO 5: The analyst evaluates the results of measurements using statistical methods, analyzes their accuracy and reliability.

6. 6

   CLO 6: The analyst interprets the results of research and prepares a report in accordance with laboratory safety regulations.

1. 1.
   Introduction. Lecture

   The subject of analytical chemistry. the essence of analytical chemistry. analytical reactions and their methods. reaction sensitivity and conditions. solutions.

2. 2.
   Reactions and analysis of first group cationsLecture

   General characteristics of first group cations. silver. mercury. lead

3. 3.
   Second group cations.Lecture

   Second group cations. general characteristics of second group cations. reactions and analysis of second group cations. barium. sequential progress of the analysis of strontium.calcium.first and second group mixtures.

4. 4.
   Group III cations.Lecture

   General characteristics of third group cations. reactions and analysis of third group cations. aluminum. chrome. zinc. tin. arsenic. sequential course of analysis of mixtures of cations of the third group.

5. 5.
   Group IV cations.Lecture

   General characteristics of fourth group cations. reactions and analysis of cations of the fourth group. iron. manganese. magnesium. bismuth. stilbum.

6. 6.
   Fifth group cations.Lecture

   General characteristics of fifth group cations. reactions and analysis of fifth group cations. copper. cadmium. divalent mercury. cobalt. nickel.

7. 7.
   Sixth analytical group cations.Lecture

   Sixth analytical group cations. general characteristics of cations of the sixth analytical group. reactions and analysis of cations of the sixth analytical group. potassium. sodium. ammonium ion.

8. 8.
   Azərbaycanda müstəqil dövlətçilik ənənələrinin bərpa edilməsi (ix-xii əsrin əvvəli)Lecture

   Azərbaycanda müstəqil dövlətçilik ənənələrinin bərpa edilməsi mövzusu ix–xi əsrlərdə hakimiyyətə gələn yerli sülalələrin siyasi fəaliyyətini və dövlət quruculuğu prosesini əhatə edir. bu dövrdə yerli hökmdarların xarici işğalçılara qarşı apardıqları mübarizə və ölkənin müstəqilliyinin qorunması istiqamətində gördükləri tədbirlər araşdırılır. mövzuda dövlət idarəçiliyinin inkişafı, inzibati quruluşun möhkəmlənməsi və hakimiyyətin təşkili məsələləri təhlil edilir. eyni zamanda, dövrün sosial, iqtisadi, siyasi və mədəni həyatı, eləcə də dövlətçiliyin inkişafına təsir göstərən amillər öyrənilir. bu mövzunun mənimsənilməsi azərbaycanın orta əsrlərdə müstəqil dövlətçilik ənənələrinin bərpası və inkişaf xüsusiyyətlərini anlamaq baxımından mühüm əhəmiyyət daşıyır.

   • • ftn4: tələbələrin ən azından minimum məlumat əldə etməsi, mövzular ətrafında öz fikrinin formalaşmasının səviyyəsi yoxlanılır.
   • • ftn3: tələbələrin bu və ya digər məsələlərlə bağlı obyektiv mövqeyini formalaşmasına nail olunur.
   • • ftn1: azərbaycan tarixinin dövrlərinin əsas mahiyyəti izah edilir.
   • • ftn2: azərbaycan tarixi üzrə bəzi mübahisəli məsələlərə aydınlıq gətirilir.
   • • ftn5: tələbələrə qədim tariximizin müasir dövrlə uzlaşdırılması vərdişləri aşılanır.
9. 9.
   Analysis of metals and alloysLecture

   Analysis of metals and alloys. analysis of non-ferrous metals and alloys.

10. 10.
    Analytical reactions of anions.Lecture

    Analytical reactions of anions. analytical reactions of first group anions (cl-, br-, i-, s2-, no2-,

11. 11.
    Quantitative chemical analysis.Lecture

    Gravimetric analysis. titrimetric analysis. determination of equivalence point. acid-base titration. titration curves. complexometric titration. oxidation-reduction titration. iodometry.

12. 12.
    Methods of chromatography and its types.Lecture

    Methods of chromatography and its types. gas chromatography. chromatographic column. chromatographic detectors. stationary phase. chromatographic peaks. the effectiveness of kalonka. phase selectivity. qualitative and quantitative analysis. application of gas chromatography in physical-chemical research. unstable phase.

13. 13.
    Gas-liquid chromatography.Lecture

    Gas-liquid chromatography. column liquid chromatography (lcc). adsorption and distributed kmx.

14. 14.
    Ir spectroscopy.Lecture

    Ir spectroscopy.

15. 15.
    Nmr spectroscopy.Lecture

    Impulse method. nuclear chemical shift and spin-spin interaction. interpretation of NMR spectra. NMR spectroscopy of 1h and 13c atoms. mass spectroscopy. ionization methods. mass analyzers. identification of molecular ion peaks.

16. 16.
    Specific reactions of sodium and potassium ionsSeminar

    Specific reactions of sodium and potassium ions

17. 17.
    Specific reactions of ammonium and magnesium ionsSeminar

    Specific reactions of ammonium and magnesium ions

18. 18.
    General characteristics of second group cationsSeminar

    General characteristics of second group cations

19. 19.
    General characteristics of third group cationsSeminar

    General characteristics of third group cations

20. 20.
    Specific reactions of fe3+ ionSeminar

    Specific reactions of fe3+ ion

21. 21.
    General characteristics of copper subgroup cationsSeminar

    Mis yarımqrupu kationlarının ümumi xarakteristikası

22. 22.
    General characteristics of cadmium subgroup cationsSeminar

    General characteristics of cadmium subgroup cations

23. 23.
    Determination of lead in solutionSeminar

    Determination of lead in solution

24. 24.
    Analytical reactions of first group anions (cl-, br-, i-, s2-, no2-, no3-).Independent work

    Analytical reactions of first group anions (cl-, br-, i-, s2-, no2-, no3-).

25. 25.
    The sequential course of the analysis of the first and second group mixtures.Independent work

    The sequential course of the analysis of the first and second group mixtures.

26. 26.
    Sequential course of analysis of mixtures of cations of the third group.Independent work

    Sequential course of analysis of mixtures of cations of the third group.

27. 27.
    Gas-liquid chromatography. column liquid chromatography (lcc).Independent work

    Gas-liquid chromatography. column liquid chromatography (lcc).

28. 28.
    Interpretation of NMR spectra. NMR spectroscopy of 1h and 13c atoms. mass spectroscopy.Independent work

    Interpretation of NMR spectra. NMR spectroscopy of 1h and 13c atoms. mass spectroscopy.

29. 29.
    The subject of analytical chemistry. the essence of analytical chemistry. analytical reactions and their methods. reaction sensitivity and conditions. solutions.Lecture

    The subject of analytical chemistry. the essence of analytical chemistry. analytical reactions and their methods. reaction sensitivity and conditions. solutions.

30. 30.
    Introduction. the subject of analytical chemistry. the essence of analytical chemistry.Lecture

    Analytical reactions and their methods. reaction sensitivity and conditions. solutions.

31. 31.
    1. introduction. relationships between analytical chemistry and industryLecture
32. 32.
    2. reactions and analysis of first group cations. general characteristics of first group cations. ammonium ion. potassium. sodium. magnesiumLecture
33. 33.
    3. second group cations. general characteristics of second group cations. reactions and analysis of second group cations. calcium. strontium. barium. the sequential course of the analysis of the first and second group mixturesLecture
34. 34.
    4. third group cations. general characteristics of third group cations. reactions and analysis of third group cations. silver. mercury. lead.. sequential progress of the analysis of mixtures of cations of the third groupLecture
35. 35.
    5. fourth group cations. general characteristics of fourth group cations. reactions and analysis of cations of the fourth group. zinc. aluminum. chrome. tinLecture
36. 36.
    6. general characteristics of fifth group cations. iron. manganese. magnesium. bismuth. stilbum reactions and analysis of group five cationsLecture
37. 37.
    7. sixth analytical group cations. general characteristics of cations of the sixth analytical group. copper. cadmium. divalent mercury. cobalt. nickel. reactions and analysis of cations of the sixth analytical groupLecture
38. 38.
    7. sixth analytical group cations. general characteristics of cations of the sixth analytical group. copper. cadmium. divalent mercury. cobalt. nickel. reactions and analysis of cations of the sixth analytical groupLecture
39. 39.
    8. ion, chromophore theory of indicators. buffer solutions. selection of indicators according to the titration curve. factors affecting stability of complex compounds: nature of ligand and metal ions, ionic radius, environment. distribution of metals among some complexesLecture
40. 40.
    9. metallurgical industry: composition of metals and alloys. analysis of metals and alloys. analysis of non-ferrous metals and alloysLecture
41. 41.
    10. analytical reactions of anions. analytical reactions of first group anions (cl-, br-, i-, s2-, no2-, no3-). analytical reactions of first-fourth group anions (so42-, so32-, s2o32-, po43-, aso43-, aso33-)Lecture
42. 42.
    11. quantitative chemical analysis. gravimetric analysis. titrimetric analysis. determination of equivalence point. acid-base titration. titration curves. complexometric titration. oxidation-reduction titration. iodometryLecture
43. 43.
    12. methods of chromatography and its types. gas chromatography. chromatographic column. chromatographic detectors. stationary phase. chromatographic peaks. the effectiveness of kalonka. phase selectivity. application of gas chromatography in physical-chemical research. unstable phaseLecture
44. 44.
    12. methods of chromatography and its types. gas chromatography. chromatographic column. chromatographic detectors. stationary phase. chromatographic peaks. the effectiveness of kalonka. phase selectivity. application of gas chromatography in physical-chemical research. unstable phaseLecture
45. 45.
    13. mass-spectroscopy. ionization methods. mass analyzers. identification of molecular ion peaksLecture
46. 46.
    13. mass-spectroscopy. ionization methods. mass analyzers. identification of molecular ion peaksLecture
47. 47.
    14. IR spectroscopy. interaction of dances. hydrogen bonding. sample preparation. interpretation of spectra. frequencies of characteristic groups of organic substancesLecture
48. 48.
    15. NMR spectroscopy. magnetic properties of nuclei. impulse method. nuclear chemical shift and spin-spin interaction. interpretation of NMR spectra. NMR spectroscopy of 1h and 13c atomsLecture
49. 49.
    15. NMR spectroscopy. magnetic properties of nuclei. impulse method. nuclear chemical shift and spin-spin interaction. interpretation of NMR spectra. NMR spectroscopy of 1h and 13c atomsLecture
50. 50.
    1. analytical reactions of first group anions (cl-, br-, i-, s2-, no2-, no3-)Seminar
51. 51.
    2. sequential course of analysis of the first and second group mixturesSeminar
52. 52.
    3. reactions and analysis of second group cations. calcium. strontium. barium. the sequential course of the analysis of the first and second group mixturesSeminar
53. 53.
    4. sequential course of analysis of mixtures of cations of the third groupSeminar

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