AZTUProgrammes

Subject · Chemical engineering

Analytical chemistry and instrumental analysisTopics

İF-30394 creditsAutumn semesterElective

Topic plan

The subject's topics and the learning outcomes attached to each one.

53 topics

  1. 1. Introduction.

    Lecture

    The subject of analytical chemistry. the essence of analytical chemistry. analytical reactions and their methods. reaction sensitivity and conditions. solutions.

    Open resource: Introduction. (opens in a new tab)

  2. 2. Reactions and analysis of first group cations

    Lecture

    General characteristics of first group cations. silver. mercury. lead

    Open resource: Reactions and analysis of first group cations (opens in a new tab)

  3. 3. Second group cations.

    Lecture

    Second group cations. general characteristics of second group cations. reactions and analysis of second group cations. barium. sequential progress of the analysis of strontium.calcium.first and second group mixtures.

    Open resource: Second group cations. (opens in a new tab)

  4. 4. Group III cations.

    Lecture

    General characteristics of third group cations. reactions and analysis of third group cations. aluminum. chrome. zinc. tin. arsenic. sequential course of analysis of mixtures of cations of the third group.

    Open resource: Group III cations. (opens in a new tab)

  5. 5. Group IV cations.

    Lecture

    General characteristics of fourth group cations. reactions and analysis of cations of the fourth group. iron. manganese. magnesium. bismuth. stilbum.

    Open resource: Group IV cations. (opens in a new tab)

  6. 6. Fifth group cations.

    Lecture

    General characteristics of fifth group cations. reactions and analysis of fifth group cations. copper. cadmium. divalent mercury. cobalt. nickel.

    Open resource: Fifth group cations. (opens in a new tab)

  7. 7. Sixth analytical group cations.

    Lecture

    Sixth analytical group cations. general characteristics of cations of the sixth analytical group. reactions and analysis of cations of the sixth analytical group. potassium. sodium. ammonium ion.

    Open resource: Sixth analytical group cations. (opens in a new tab)

  8. 8. Azərbaycanda müstəqil dövlətçilik ənənələrinin bərpa edilməsi (ix-xii əsrin əvvəli)

    Lecture

    Azərbaycanda müstəqil dövlətçilik ənənələrinin bərpa edilməsi mövzusu ix–xi əsrlərdə hakimiyyətə gələn yerli sülalələrin siyasi fəaliyyətini və dövlət quruculuğu prosesini əhatə edir. bu dövrdə yerli hökmdarların xarici işğalçılara qarşı apardıqları mübarizə və ölkənin müstəqilliyinin qorunması istiqamətində gördükləri tədbirlər araşdırılır. mövzuda dövlət idarəçiliyinin inkişafı, inzibati quruluşun möhkəmlənməsi və hakimiyyətin təşkili məsələləri təhlil edilir. eyni zamanda, dövrün sosial, iqtisadi, siyasi və mədəni həyatı, eləcə də dövlətçiliyin inkişafına təsir göstərən amillər öyrənilir. bu mövzunun mənimsənilməsi azərbaycanın orta əsrlərdə müstəqil dövlətçilik ənənələrinin bərpası və inkişaf xüsusiyyətlərini anlamaq baxımından mühüm əhəmiyyət daşıyır.

    Topic learning outcomes

    • • ftn4: tələbələrin ən azından minimum məlumat əldə etməsi, mövzular ətrafında öz fikrinin formalaşmasının səviyyəsi yoxlanılır.
    • • ftn3: tələbələrin bu və ya digər məsələlərlə bağlı obyektiv mövqeyini formalaşmasına nail olunur.
    • • ftn1: azərbaycan tarixinin dövrlərinin əsas mahiyyəti izah edilir.
    • • ftn2: azərbaycan tarixi üzrə bəzi mübahisəli məsələlərə aydınlıq gətirilir.
    • • ftn5: tələbələrə qədim tariximizin müasir dövrlə uzlaşdırılması vərdişləri aşılanır.

  9. 9. Analysis of metals and alloys

    Lecture

    Analysis of metals and alloys. analysis of non-ferrous metals and alloys.

    Open resource: Analysis of metals and alloys (opens in a new tab)

  10. 10. Analytical reactions of anions.

    Lecture

    Analytical reactions of anions. analytical reactions of first group anions (cl-, br-, i-, s2-, no2-,

    Open resource: Analytical reactions of anions. (opens in a new tab)

  11. 11. Quantitative chemical analysis.

    Lecture

    Gravimetric analysis. titrimetric analysis. determination of equivalence point. acid-base titration. titration curves. complexometric titration. oxidation-reduction titration. iodometry.

    Open resource: Quantitative chemical analysis. (opens in a new tab)

  12. 12. Methods of chromatography and its types.

    Lecture

    Methods of chromatography and its types. gas chromatography. chromatographic column. chromatographic detectors. stationary phase. chromatographic peaks. the effectiveness of kalonka. phase selectivity. qualitative and quantitative analysis. application of gas chromatography in physical-chemical research. unstable phase.

    Open resource: Methods of chromatography and its types. (opens in a new tab)

  13. 13. Gas-liquid chromatography.

    Lecture

    Gas-liquid chromatography. column liquid chromatography (lcc). adsorption and distributed kmx.

    Open resource: Gas-liquid chromatography. (opens in a new tab)

  14. 14. Ir spectroscopy.

    Lecture

    Ir spectroscopy.

    Open resource: Ir spectroscopy. (opens in a new tab)

  15. 15. Nmr spectroscopy.

    Lecture

    Impulse method. nuclear chemical shift and spin-spin interaction. interpretation of NMR spectra. NMR spectroscopy of 1h and 13c atoms. mass spectroscopy. ionization methods. mass analyzers. identification of molecular ion peaks.

    Open resource: Nmr spectroscopy. (opens in a new tab)

  16. 16. Specific reactions of sodium and potassium ions

    Seminar

    Specific reactions of sodium and potassium ions

    Open resource: Specific reactions of sodium and potassium ions (opens in a new tab)

  17. 17. Specific reactions of ammonium and magnesium ions

    Seminar

    Specific reactions of ammonium and magnesium ions

    Open resource: Specific reactions of ammonium and magnesium ions (opens in a new tab)

  18. 18. General characteristics of second group cations

    Seminar

    General characteristics of second group cations

    Open resource: General characteristics of second group cations (opens in a new tab)

  19. 19. General characteristics of third group cations

    Seminar

    General characteristics of third group cations

    Open resource: General characteristics of third group cations (opens in a new tab)

  20. 20. Specific reactions of fe3+ ion

    Seminar

    Specific reactions of fe3+ ion

    Open resource: Specific reactions of fe3+ ion (opens in a new tab)

  21. 21. General characteristics of copper subgroup cations

    Seminar

    Mis yarımqrupu kationlarının ümumi xarakteristikası

    Open resource: General characteristics of copper subgroup cations (opens in a new tab)

  22. 22. General characteristics of cadmium subgroup cations

    Seminar

    General characteristics of cadmium subgroup cations

    Open resource: General characteristics of cadmium subgroup cations (opens in a new tab)

  23. 23. Determination of lead in solution

    Seminar

    Determination of lead in solution

    Open resource: Determination of lead in solution (opens in a new tab)

  24. 24. Analytical reactions of first group anions (cl-, br-, i-, s2-, no2-, no3-).

    Independent work

    Analytical reactions of first group anions (cl-, br-, i-, s2-, no2-, no3-).

    Open resource: Analytical reactions of first group anions (cl-, br-, i-, s2-, no2-, no3-). (opens in a new tab)

  25. 25. The sequential course of the analysis of the first and second group mixtures.

    Independent work

    The sequential course of the analysis of the first and second group mixtures.

    Open resource: The sequential course of the analysis of the first and second group mixtures. (opens in a new tab)

  26. 26. Sequential course of analysis of mixtures of cations of the third group.

    Independent work

    Sequential course of analysis of mixtures of cations of the third group.

    Open resource: Sequential course of analysis of mixtures of cations of the third group. (opens in a new tab)

  27. 27. Gas-liquid chromatography. column liquid chromatography (lcc).

    Independent work

    Gas-liquid chromatography. column liquid chromatography (lcc).

    Open resource: Gas-liquid chromatography. column liquid chromatography (lcc). (opens in a new tab)

  28. 28. Interpretation of NMR spectra. NMR spectroscopy of 1h and 13c atoms. mass spectroscopy.

    Independent work

    Interpretation of NMR spectra. NMR spectroscopy of 1h and 13c atoms. mass spectroscopy.

    Open resource: Interpretation of NMR spectra. NMR spectroscopy of 1h and 13c atoms. mass spectroscopy. (opens in a new tab)

  29. 29. The subject of analytical chemistry. the essence of analytical chemistry. analytical reactions and their methods. reaction sensitivity and conditions. solutions.

    Lecture

    The subject of analytical chemistry. the essence of analytical chemistry. analytical reactions and their methods. reaction sensitivity and conditions. solutions.

    Open resource: The subject of analytical chemistry. the essence of analytical chemistry. analytical reactions and their methods. reaction sensitivity and conditions. solutions. (opens in a new tab)

  30. 30. Introduction. the subject of analytical chemistry. the essence of analytical chemistry.

    Lecture

    Analytical reactions and their methods. reaction sensitivity and conditions. solutions.

    Open resource: Introduction. the subject of analytical chemistry. the essence of analytical chemistry. (opens in a new tab)

  31. 31. 1. introduction. relationships between analytical chemistry and industry

    Lecture

  32. 32. 2. reactions and analysis of first group cations. general characteristics of first group cations. ammonium ion. potassium. sodium. magnesium

    Lecture

  33. 33. 3. second group cations. general characteristics of second group cations. reactions and analysis of second group cations. calcium. strontium. barium. the sequential course of the analysis of the first and second group mixtures

    Lecture

  34. 34. 4. third group cations. general characteristics of third group cations. reactions and analysis of third group cations. silver. mercury. lead.. sequential progress of the analysis of mixtures of cations of the third group

    Lecture

  35. 35. 5. fourth group cations. general characteristics of fourth group cations. reactions and analysis of cations of the fourth group. zinc. aluminum. chrome. tin

    Lecture

  36. 36. 6. general characteristics of fifth group cations. iron. manganese. magnesium. bismuth. stilbum reactions and analysis of group five cations

    Lecture

  37. 37. 7. sixth analytical group cations. general characteristics of cations of the sixth analytical group. copper. cadmium. divalent mercury. cobalt. nickel. reactions and analysis of cations of the sixth analytical group

    Lecture

  38. 38. 7. sixth analytical group cations. general characteristics of cations of the sixth analytical group. copper. cadmium. divalent mercury. cobalt. nickel. reactions and analysis of cations of the sixth analytical group

    Lecture

  39. 39. 8. ion, chromophore theory of indicators. buffer solutions. selection of indicators according to the titration curve. factors affecting stability of complex compounds: nature of ligand and metal ions, ionic radius, environment. distribution of metals among some complexes

    Lecture

  40. 40. 9. metallurgical industry: composition of metals and alloys. analysis of metals and alloys. analysis of non-ferrous metals and alloys

    Lecture

  41. 41. 10. analytical reactions of anions. analytical reactions of first group anions (cl-, br-, i-, s2-, no2-, no3-). analytical reactions of first-fourth group anions (so42-, so32-, s2o32-, po43-, aso43-, aso33-)

    Lecture

  42. 42. 11. quantitative chemical analysis. gravimetric analysis. titrimetric analysis. determination of equivalence point. acid-base titration. titration curves. complexometric titration. oxidation-reduction titration. iodometry

    Lecture

  43. 43. 12. methods of chromatography and its types. gas chromatography. chromatographic column. chromatographic detectors. stationary phase. chromatographic peaks. the effectiveness of kalonka. phase selectivity. application of gas chromatography in physical-chemical research. unstable phase

    Lecture

  44. 44. 12. methods of chromatography and its types. gas chromatography. chromatographic column. chromatographic detectors. stationary phase. chromatographic peaks. the effectiveness of kalonka. phase selectivity. application of gas chromatography in physical-chemical research. unstable phase

    Lecture

  45. 45. 13. mass-spectroscopy. ionization methods. mass analyzers. identification of molecular ion peaks

    Lecture

  46. 46. 13. mass-spectroscopy. ionization methods. mass analyzers. identification of molecular ion peaks

    Lecture

  47. 47. 14. IR spectroscopy. interaction of dances. hydrogen bonding. sample preparation. interpretation of spectra. frequencies of characteristic groups of organic substances

    Lecture

  48. 48. 15. NMR spectroscopy. magnetic properties of nuclei. impulse method. nuclear chemical shift and spin-spin interaction. interpretation of NMR spectra. NMR spectroscopy of 1h and 13c atoms

    Lecture

  49. 49. 15. NMR spectroscopy. magnetic properties of nuclei. impulse method. nuclear chemical shift and spin-spin interaction. interpretation of NMR spectra. NMR spectroscopy of 1h and 13c atoms

    Lecture

  50. 50. 1. analytical reactions of first group anions (cl-, br-, i-, s2-, no2-, no3-)

    Seminar

  51. 51. 2. sequential course of analysis of the first and second group mixtures

    Seminar

  52. 52. 3. reactions and analysis of second group cations. calcium. strontium. barium. the sequential course of the analysis of the first and second group mixtures

    Seminar

  53. 53. 4. sequential course of analysis of mixtures of cations of the third group

    Seminar