Materialların struktur analiz metodlarıSyllabus

Subject code

İFS-3275y

Credits

6

Student workload

180

Semester

Autumn semester

Academic year

2025-2026

Subject type

Elective

Form of education

Full-time

Language of instruction

Azerbaijani

In-class hours

a) 30 saat – mühazirə; b) 15 saat – laboratoriya; c) 15 saat – məşğələ

Out-of-class hours

a) 72 saat – sərbəst iş; b) 48 saat – hazırlıq

Metalların makrostruktur tədqiqat üsullarını; metalların mikrostruktur tədqiqat üsullarını; i̇şıqkeçirən elektron mikroskop üsulunu; rastrov elektron mikroskop üsulunu; rentgenstruktur analizin əsas üsullarını öyrənmələrini ehtiva edir

• lecture
• laboratory work
• seminar
• interactive discussion
• presentations

1. 1

   CLO 1: Students will master modern instrumental methods for determining the microstructure, phase composition, and crystal lattice parameters of metals and advanced alloys. they will gain an in-depth understanding of the working principles of optical and electron microscopy (sem, tem) as well as x-ray structure analysis (xrd) equipment. accurate diagnosis of intermetallic phases, nanostructures and intermediate layers formed in materials with especially complex composition (for example, 5 or more components with high entropy) will be carried out. finally, students will be able to quantify the relationship between the structure and mechanical properties of the material by deciphering the obtained spectral and visual data.

2. 2

   CLO 2: This subject examines the physico-chemical nature of non-ferrous metals such as aluminum, copper, titanium and magnesium, as well as their multicomponent alloys. students will analyze the specific phase transformations that occur in non-ferrous alloys, including the mechanisms of natural and artificial wear (dispersion hardening) processes. they will learn to design the required homogenizing heating or tempering regimes to optimize the properties of the part according to the industrial application. at the end of the subject, the ability to detect and eliminate thermal processing defects of special-purpose nonferrous materials used in the aerospace and electronics industries will be developed.

1. 1.
   Research methods of macro and microstructureLecture

   Methodology for studying the structure of materials at both the macroscopic and microscopic level.

2. 2.
   Classification of methods of studying the structure of metalsLecture

   General classification of modern research methods used to study the internal structure and properties of metals

3. 3.
   Study of macrostructureLecture

   Determination of macrostructural defects by looking at fractures and cuts of metals with the naked eye or with low magnification.

4. 4.
   Study of microstructure (microanalysis)Lecture

   Refinement of the grain structure, phases and microscopic defects of metals through a microscope

5. 5.
   Transmission electron microscopeLecture

   Working principle, structure and capabilities of transmission electron microscopes (tem).

6. 6.
   Research methods of metals and alloys by transmission electron microscopy.Lecture

   The method of studying dislocations, nano-phases in metals and alloys with a transmission electron microscope.

7. 7.
   Research methods of metals and alloys by transmission electron microscopy

   The method of studying dislocations, nano-phases in metals and alloys with a transmission electron microscope

8. 8.
   Raster electron microscopeLecture

   The structure, working principle and role of the scanning electron microscope (sem) in the study of surface topography

9. 9.
   Research methods of metals with the help of REMLecture

   Study of fracture surfaces (fractography) and morphology of metals by means of raster electron microscope (rem).

10. 10.
    X-ray structural analysis in the study of metallic materials.Lecture

    The method of studying the crystalline structure of metals based on x-ray diffraction

11. 11.
    Basic concepts and formulas of crystallography. structure of crystals.Lecture

    Study of crystal lattices, syngonias, miller indices and geometric properties of crystals.

12. 12.
    Analysis of the structural state of metallic materialsLecture

    Study of the changes in the structure of metallic materials and the resulting stresses after thermal and mechanical processing

13. 13.
    Structure of x-ray spectral microanalyzerLecture

    Optical and electronic structure of x-ray spectral microanalyzers performing local chemical analysis.

14. 14.
    Basic settingsLecture

    Study of the main parameters that determine the accuracy and sensitivity of devices and tests in structural analysis methods.

1. Gulyaev a.p. metallurgy. moscow. 2012.